国家药典委于2024年7月26日发布了完善版的《0212药材和饮片检定通则标准草案公示稿》和《2341 农药残留量测定法标准草案公示稿》,引起了行业内的关注和重视。
新增11种中药材的36种限用农药清单。通则2341中农残测定方法也发生了很大变化。面对这样的变化与挑战,莱奥已建立整体解决方案,以助力相关机构及企业从容应对。
[/fusion_text][fusion_table fusion_table_type=”2″ fusion_table_rows=”6″ fusion_table_columns=”2″ animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility”]| 《2020版药典》2341通则 | 新版2341通则(公示稿) |
|---|---|
| 第一法 有机氯类农药残留量测定法 | 第一法 药材及饮片(植物类)中禁用农药多残留测定法 |
| 第二法 有机磷类农药残留量测定法 | 第二法 相关药材及饮片品种中农药多残留测定法(新增) |
| 第三法 拟除虫菊酯类农药残留量测定法 | 第三法 药材及饮片中二硫代氨基甲酸盐类农药残留量测定法(新增) |
| 第四法 农药多残留量测定法 | 第四法 农药多残留量测定法(质谱法) |
| 第五法 药材及饮片(植物类)中禁用农药多残留测定法 |
莱奥针对“第一法 药材及饮片(植物类)中禁用农药多残留测定法”前处理提供完整的解决方案。
[/fusion_text][fusion_title title_type=”text” scroll_reveal_effect=”color_change” scroll_reveal_basis=”chars” scroll_reveal_behavior=”always” scroll_reveal_duration=”500″ scroll_reveal_stagger=”200″ scroll_reveal_delay=”0″ scroll_reveal_above_fold=”yes” marquee_direction=”left” marquee_mask_edges=”no” marquee_speed=”15000″ rotation_effect=”bounceIn” display_time=”1200″ highlight_effect=”circle” loop_animation=”once” highlight_animation_duration=”1500″ highlight_width=”9″ highlight_smudge_effect=”no” highlight_top_margin=”0″ title_link=”off” link_target=”_self” content_align=”left” size=”div” text_shadow=”no” text_shadow_blur=”0″ text_stroke=”no” text_stroke_size=”1″ text_overflow=”none” gradient_font=”no” gradient_start_position=”0″ gradient_end_position=”100″ gradient_type=”linear” radial_direction=”center center” linear_angle=”180″ style_type=”default” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” font_size=”26″ fusion_font_variant_title_font=”600″ fusion_font_family_title_font=”Montserrat” margin_bottom=”30px” margin_top=”30px”]一、仪器设备
[/fusion_title][fusion_builder_row_inner][fusion_builder_column_inner type=”1_3″ type=”1_3″ align_self=”auto” content_layout=”column” align_content=”flex-start” valign_content=”flex-start” content_wrap=”wrap” center_content=”no” column_tag=”div” target=”_self” hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” order_medium=”0″ order_small=”0″ hover_type=”none” border_style=”solid” box_shadow=”no” box_shadow_blur=”0″ box_shadow_spread=”0″ background_type=”single” gradient_start_position=”0″ gradient_end_position=”100″ gradient_type=”linear” radial_direction=”center center” linear_angle=”180″ lazy_load=”avada” background_position=”left top” background_repeat=”no-repeat” background_blend_mode=”none” background_slider_skip_lazy_loading=”no” background_slider_loop=”yes” background_slider_pause_on_hover=”no” background_slider_slideshow_speed=”5000″ background_slider_animation=”fade” background_slider_direction=”up” 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filter_sepia_hover=”0″ filter_opacity_hover=”100″ filter_blur_hover=”0″ image_id=”6065|fusion-400″ link=”https://leowlab.com/positive-pressure-solid-phase-extractor/purifier-a48/” caption_title=”Leowlab Purifier A48″ caption_text=”48位正压固相萃取仪” caption_title_transform=”capitalize” caption_text_transform=”capitalize” caption_overlay_color=”hsla(var(–awb-color7-h),var(–awb-color7-s),calc(var(–awb-color7-l) + 40%),var(–awb-color7-a))” fusion_font_variant_caption_title_font=”600″ fusion_font_family_caption_title_font=”Montserrat” caption_title_size=”16″ caption_title_color=”var(–awb-color1)” fusion_font_variant_caption_text_font=”400″ fusion_font_family_caption_text_font=”Montserrat” caption_text_size=”16″ caption_border_color=”var(–awb-color1)” caption_text_color=”var(–awb-color1)”]https://leowlab.com/wp-content/uploads/2025/10/A48-400×400.jpg[/fusion_imageframe][/fusion_builder_column_inner][fusion_builder_column_inner type=”1_3″ type=”1_3″ align_self=”auto” content_layout=”column” align_content=”flex-start” valign_content=”flex-start” content_wrap=”wrap” center_content=”no” column_tag=”div” target=”_self” hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” order_medium=”0″ order_small=”0″ hover_type=”none” border_style=”solid” box_shadow=”no” box_shadow_blur=”0″ box_shadow_spread=”0″ background_type=”single” gradient_start_position=”0″ gradient_end_position=”100″ gradient_type=”linear” radial_direction=”center center” linear_angle=”180″ lazy_load=”avada” background_position=”left top” background_repeat=”no-repeat” background_blend_mode=”none” background_slider_skip_lazy_loading=”no” background_slider_loop=”yes” background_slider_pause_on_hover=”no” background_slider_slideshow_speed=”5000″ background_slider_animation=”fade” background_slider_direction=”up” background_slider_animation_speed=”800″ sticky=”off” sticky_devices=”small-visibility,medium-visibility,large-visibility” absolute=”off” filter_type=”regular” filter_hover_element=”self” filter_hue=”0″ filter_saturation=”100″ filter_brightness=”100″ filter_contrast=”100″ filter_invert=”0″ filter_sepia=”0″ filter_opacity=”100″ filter_blur=”0″ filter_hue_hover=”0″ filter_saturation_hover=”100″ filter_brightness_hover=”100″ filter_contrast_hover=”100″ filter_invert_hover=”0″ filter_sepia_hover=”0″ filter_opacity_hover=”100″ filter_blur_hover=”0″ transform_type=”regular” transform_hover_element=”self” transform_scale_x=”1″ transform_scale_y=”1″ transform_translate_x=”0″ transform_translate_y=”0″ transform_rotate=”0″ transform_skew_x=”0″ transform_skew_y=”0″ transform_scale_x_hover=”1″ transform_scale_y_hover=”1″ transform_translate_x_hover=”0″ transform_translate_y_hover=”0″ transform_rotate_hover=”0″ transform_skew_x_hover=”0″ transform_skew_y_hover=”0″ transition_duration=”300″ transition_easing=”ease” scroll_motion_devices=”small-visibility,medium-visibility,large-visibility” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ last=”no” border_position=”all”][fusion_imageframe custom_aspect_ratio=”100″ lightbox=”no” linktarget=”_blank” align_medium=”none” align_small=”none” align=”center” hover_type=”none” magnify_duration=”120″ scroll_height=”100″ scroll_speed=”1″ caption_style=”resa” caption_align_medium=”none” caption_align_small=”none” caption_align=”center” caption_title_tag=”div” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” filter_hue=”0″ filter_saturation=”100″ filter_brightness=”100″ filter_contrast=”100″ filter_invert=”0″ filter_sepia=”0″ filter_opacity=”100″ filter_blur=”0″ filter_hue_hover=”0″ filter_saturation_hover=”100″ filter_brightness_hover=”100″ filter_contrast_hover=”100″ filter_invert_hover=”0″ filter_sepia_hover=”0″ filter_opacity_hover=”100″ filter_blur_hover=”0″ image_id=”6069|fusion-400″ link=”https://leowlab.com/nitrogen-evaporator/smartvap-ae/” caption_title=”Leowlab SmartVap AE” caption_title_transform=”capitalize” caption_text_transform=”capitalize” caption_overlay_color=”hsla(var(–awb-color7-h),var(–awb-color7-s),calc(var(–awb-color7-l) + 40%),var(–awb-color7-a))” fusion_font_variant_caption_title_font=”600″ fusion_font_family_caption_title_font=”Montserrat” caption_title_size=”16″ caption_title_color=”var(–awb-color1)” fusion_font_variant_caption_text_font=”400″ fusion_font_family_caption_text_font=”Montserrat” caption_text_size=”16″ caption_border_color=”var(–awb-color1)” caption_text=”全自动氮吹浓缩仪”]https://leowlab.com/wp-content/uploads/2025/10/QE-AE-400×400.jpg[/fusion_imageframe][/fusion_builder_column_inner][fusion_builder_column_inner type=”1_3″ type=”1_3″ align_self=”auto” content_layout=”column” align_content=”flex-start” valign_content=”flex-start” content_wrap=”wrap” center_content=”no” column_tag=”div” target=”_self” hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” order_medium=”0″ order_small=”0″ hover_type=”none” border_style=”solid” box_shadow=”no” box_shadow_blur=”0″ box_shadow_spread=”0″ background_type=”single” gradient_start_position=”0″ gradient_end_position=”100″ gradient_type=”linear” radial_direction=”center center” linear_angle=”180″ lazy_load=”avada” background_position=”left top” background_repeat=”no-repeat” background_blend_mode=”none” background_slider_skip_lazy_loading=”no” background_slider_loop=”yes” background_slider_pause_on_hover=”no” background_slider_slideshow_speed=”5000″ background_slider_animation=”fade” background_slider_direction=”up” background_slider_animation_speed=”800″ sticky=”off” sticky_devices=”small-visibility,medium-visibility,large-visibility” absolute=”off” filter_type=”regular” filter_hover_element=”self” filter_hue=”0″ filter_saturation=”100″ filter_brightness=”100″ filter_contrast=”100″ filter_invert=”0″ filter_sepia=”0″ filter_opacity=”100″ filter_blur=”0″ filter_hue_hover=”0″ filter_saturation_hover=”100″ filter_brightness_hover=”100″ filter_contrast_hover=”100″ filter_invert_hover=”0″ filter_sepia_hover=”0″ filter_opacity_hover=”100″ filter_blur_hover=”0″ transform_type=”regular” transform_hover_element=”self” transform_scale_x=”1″ transform_scale_y=”1″ transform_translate_x=”0″ transform_translate_y=”0″ transform_rotate=”0″ transform_skew_x=”0″ transform_skew_y=”0″ transform_scale_x_hover=”1″ transform_scale_y_hover=”1″ transform_translate_x_hover=”0″ transform_translate_y_hover=”0″ transform_rotate_hover=”0″ transform_skew_x_hover=”0″ transform_skew_y_hover=”0″ transition_duration=”300″ transition_easing=”ease” scroll_motion_devices=”small-visibility,medium-visibility,large-visibility” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ last=”no” border_position=”all”][fusion_imageframe custom_aspect_ratio=”100″ lightbox=”no” linktarget=”_blank” align_medium=”none” align_small=”none” align=”center” hover_type=”none” magnify_duration=”120″ scroll_height=”100″ scroll_speed=”1″ caption_style=”resa” caption_align_medium=”none” caption_align_small=”none” caption_align=”center” caption_title_tag=”div” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” filter_hue=”0″ filter_saturation=”100″ filter_brightness=”100″ filter_contrast=”100″ filter_invert=”0″ filter_sepia=”0″ filter_opacity=”100″ filter_blur=”0″ filter_hue_hover=”0″ filter_saturation_hover=”100″ filter_brightness_hover=”100″ filter_contrast_hover=”100″ filter_invert_hover=”0″ filter_sepia_hover=”0″ filter_opacity_hover=”100″ filter_blur_hover=”0″ image_id=”6071|fusion-400″ link=”https://leowlab.com/nitrogen-generator/nitrogen-evaporator-1/clart-mp-series/” caption_title=”Leowlab NG-MP” caption_text=”氮吹用氮气发生器” caption_title_transform=”capitalize” caption_text_transform=”capitalize” caption_overlay_color=”hsla(var(–awb-color7-h),var(–awb-color7-s),calc(var(–awb-color7-l) + 40%),var(–awb-color7-a))” fusion_font_variant_caption_title_font=”600″ fusion_font_family_caption_title_font=”Montserrat” caption_title_size=”16″ caption_title_color=”var(–awb-color1)” fusion_font_variant_caption_text_font=”400″ fusion_font_family_caption_text_font=”Montserrat” caption_text_size=”16″ caption_border_color=”var(–awb-color1)”]https://leowlab.com/wp-content/uploads/2025/10/氮发-中-400×400.jpg[/fusion_imageframe][/fusion_builder_column_inner][/fusion_builder_row_inner][fusion_table fusion_table_type=”2″ fusion_table_rows=”4″ fusion_table_columns=”2″ animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility”]| 前处理仪器设备 | |
|---|---|
| 减压涡旋浓缩仪 | 涡旋旋蒸仪 |
| 固相萃取仪 | Purifier A48 48位正压固相萃取仪 |
| 氮吹仪 | SmartVap AE 48位氮吹浓缩仪 |
| 分析仪器 | |
|---|---|
| 气相质谱仪 | 带ESI离子源 |
二、根据标准中4.3固相萃取法(方式三)的实验流程
[/fusion_title][fusion_imageframe custom_aspect_ratio=”100″ lightbox=”no” linktarget=”_self” align_medium=”none” align_small=”none” align=”center” hover_type=”none” magnify_duration=”120″ scroll_height=”100″ scroll_speed=”1″ caption_style=”off” caption_align_medium=”none” caption_align_small=”none” caption_align=”none” caption_title_tag=”2″ animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” filter_hue=”0″ filter_saturation=”100″ filter_brightness=”100″ filter_contrast=”100″ filter_invert=”0″ filter_sepia=”0″ filter_opacity=”100″ filter_blur=”0″ filter_hue_hover=”0″ filter_saturation_hover=”100″ filter_brightness_hover=”100″ filter_contrast_hover=”100″ filter_invert_hover=”0″ filter_sepia_hover=”0″ filter_opacity_hover=”100″ filter_blur_hover=”0″ image_id=”7461|full”]https://leowlab.com/wp-content/uploads/2026/01/药典农残.png[/fusion_imageframe][fusion_title title_type=”text” scroll_reveal_effect=”color_change” scroll_reveal_basis=”chars” scroll_reveal_behavior=”always” scroll_reveal_duration=”500″ scroll_reveal_stagger=”200″ scroll_reveal_delay=”0″ scroll_reveal_above_fold=”yes” marquee_direction=”left” marquee_mask_edges=”no” marquee_speed=”15000″ rotation_effect=”bounceIn” display_time=”1200″ highlight_effect=”circle” loop_animation=”once” highlight_animation_duration=”1500″ highlight_width=”9″ highlight_smudge_effect=”no” highlight_top_margin=”0″ title_link=”off” link_target=”_self” content_align=”left” size=”div” text_shadow=”no” text_shadow_blur=”0″ text_stroke=”no” text_stroke_size=”1″ text_overflow=”none” gradient_font=”no” gradient_start_position=”0″ gradient_end_position=”100″ gradient_type=”linear” radial_direction=”center center” linear_angle=”180″ style_type=”default” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” font_size=”26″ fusion_font_variant_title_font=”600″ fusion_font_family_title_font=”Montserrat” margin_bottom=”30px” margin_top=”30px”]三、实验步骤概要
[/fusion_title][fusion_text animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ disable_idd=”no” hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” fusion_font_variant_text_font=”400″ fusion_font_family_text_font=”Montserrat”]1、取粉末5g,加NaCl1g,加入乙腈50ml提取2次,合并提取液,减压浓缩至5~10ml,乙腈稀释至25ml。
2、根据标准中4.3固相萃取法(方式三):量取浓缩后提取液2ml,用Purifier A48 48位正压固相萃取仪净化样本。
3、收集后的洗脱液,和架子一起转移至SmartVap AE 48位氮吹浓缩仪,浓缩近干,用乙腈复溶2ml,待上机。
[/fusion_text][fusion_title title_type=”text” scroll_reveal_effect=”color_change” scroll_reveal_basis=”chars” scroll_reveal_behavior=”always” scroll_reveal_duration=”500″ scroll_reveal_stagger=”200″ scroll_reveal_delay=”0″ scroll_reveal_above_fold=”yes” marquee_direction=”left” marquee_mask_edges=”no” marquee_speed=”15000″ rotation_effect=”bounceIn” display_time=”1200″ highlight_effect=”circle” loop_animation=”once” highlight_animation_duration=”1500″ highlight_width=”9″ highlight_smudge_effect=”no” highlight_top_margin=”0″ title_link=”off” link_target=”_self” content_align=”left” size=”div” text_shadow=”no” text_shadow_blur=”0″ text_stroke=”no” text_stroke_size=”1″ text_overflow=”none” gradient_font=”no” gradient_start_position=”0″ gradient_end_position=”100″ gradient_type=”linear” radial_direction=”center center” linear_angle=”180″ style_type=”default” animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” font_size=”26″ fusion_font_variant_title_font=”600″ fusion_font_family_title_font=”Montserrat” margin_bottom=”30px” margin_top=”30px”]四、仪器方法优势
[/fusion_title][fusion_text animation_direction=”left” animation_speed=”0.3″ animation_delay=”0″ disable_idd=”no” hide_on_mobile=”small-visibility,medium-visibility,large-visibility” sticky_display=”normal,sticky” fusion_font_variant_text_font=”400″ fusion_font_family_text_font=”Montserrat”]1、流速可控,回收率佳:过柱时候,速度需要控制1ml/min,Leowlab Purifier A48 48正压固相萃取仪可通过调节压力,准确控制流速。2、批量大,效率高:样品量最大可兼容48批次,同时过柱及氮吹,节省实验时间。
3、固相兼容氮吹,无需转移:过柱后样品架可直接转移到Leowlab SmartVap AE 48位全自动氮吹浓缩仪,避免转移带来的损失。
4、涡旋斜吹技术:Leowlab SmartVap AE 48位全自动氮吹浓缩仪,采用斜吹技术,可更加快速,平和、防飞溅的基础上,很好的完成氮吹。
5、筛选氮吹针误差测试,保证平行性:Leowlab SmartVap AE 48位全自动氮吹浓缩仪的氮吹针经过针与针直接误差测试,层层筛选过,保证氮吹样品的平行性。
6、氮吹不跟随液面下降:Leowlab SmartVap AE 48位全自动氮吹浓缩仪不跟随液面下降,防止样品交叉污染。
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